| Attribute Name -- Attribute Label |
Unit |
Attribute definition |
datetime
--
Date and Time
|
not mapped |
The date and time |
|
Method
(Sampling/processing description of the values of
this attribute by one ore more steps.)
|
|
--- Step
1
---
|
|
Title
:
|
Date daily (YYYY-MM-DD) |
|
Description
:
|
Date daily (YYYY-MM-DD) |
|
|
PlotID
--
ID of the plot
|
no unit |
ID of the plot |
|
Method
(Sampling/processing description of the values of
this attribute by one ore more steps.)
|
|
--- Step
1
---
|
|
Title
:
|
Plot ID in Bombuscaro |
|
Description
:
|
Plot ID in Bombuscaro |
|
|
PCP
--
precipitation
|
Millimeter |
precipitation independent of the measuerement hight |
|
Method
(Sampling/processing description of the values of
this attribute by one ore more steps.)
|
|
--- Step
1
---
|
|
Title
:
|
Measurement of precipitation with totalizators |
|
Description
:
|
Measurement of weekly precipitation with five replicate totalizators (PE) having a diameter of 118 mm. |
|
Instrumentation:
|
Instrument:
Description: Auxiliary precipitation totalizator made of PET
|
Instrument: Precipitation totalizator
|
Vendor: Self-made
|
|
|
|
ECw_pcp
--
Electrical conductivity measured in precipitation
|
Microsiemens per centimeter |
Electrical conductivity measured in precipitation time series |
|
Method
(Sampling/processing description of the values of
this attribute by one ore more steps.)
|
|
--- Step
1
---
|
|
Title
:
|
Measurement of electrical conductivity |
|
Description
:
|
Measurement of electrical conductivity with conductivity measurement cell and handheld conductivity meter. |
|
Instrumentation:
|
Instrument:
Description: WTW Cond 315i handheld device coupled with TetraCon 325 conductivity cell
|
Instrument: WTW Cond 315i / TetraCon 325
|
Vendor: WTW
|
|
|
|
PHw_pcp
--
PH measured in precipitation
|
Unitless |
PH measured in precipitation time series |
|
Method
(Sampling/processing description of the values of
this attribute by one ore more steps.)
|
|
--- Step
1
---
|
|
Title
:
|
Measurement of pH values |
|
Description
:
|
Measurement of pH values with glass electrode coupled to a handheld measurement device. |
|
Instrumentation:
|
Instrument:
Description: WTW pH 330i handheld device coupled with pH glass electrode Sentix 81
|
Instrument: WTW pH 330i / Sentix 81
|
Vendor: WTW
|
|
|
|
Alw_pcp
--
Aluminium measured in precipitation
|
Milligram per liter |
Aluminium measured in precipitation time series |
|
Method
(Sampling/processing description of the values of
this attribute by one ore more steps.)
|
|
--- Step
1
---
|
|
Title
:
|
Measurement of aluminium concentrations |
|
Description
:
|
Aluminium concentrations measured by ICP-MS / ICP-OES / AAS (graphite furnace) |
|
Instrumentation:
|
Instrument:
Description:
|
Instrument: ICP-MS
|
Vendor: Agilent
|
|
|
Instrumentation:
|
Instrument:
Description:
|
Instrument: ICP-OES
|
Vendor: Agilent
|
|
|
Instrumentation:
|
Instrument:
Description:
|
Instrument: Atom Absorption Spectrometer
|
Vendor: AnalyticJena
|
|
|
|
Mnw_pcp
--
Manganese measured in precipitation
|
Milligram per liter |
Manganese measured in precipitation time series |
|
Method
(Sampling/processing description of the values of
this attribute by one ore more steps.)
|
|
--- Step
1
---
|
|
Title
:
|
Measurement of manganese concentrations |
|
Description
:
|
Manganese measured by ICP-MS |
|
Instrumentation:
|
Instrument:
Description:
|
Instrument: ICP-MS
|
Vendor: Agilent
|
|
|
|
Znw_pcp
--
Zinc measured in precipitation
|
Milligram per liter |
Zinc measured in precipitation time series |
|
Method
(Sampling/processing description of the values of
this attribute by one ore more steps.)
|
|
--- Step
1
---
|
|
Title
:
|
Measurement of zinc concentrations |
|
Description
:
|
Zinc concentrations measured by ICP-MS |
|
Instrumentation:
|
Instrument:
Description:
|
Instrument: ICP-MS
|
Vendor: Agilent
|
|
|
|
Caw_pcp
--
Calcium measured in precipitation
|
Milligram per liter |
Calcium measured in precipitation time series |
|
Method
(Sampling/processing description of the values of
this attribute by one ore more steps.)
|
|
--- Step
1
---
|
|
Title
:
|
Measurement of calcium concentrations by ICP-OES |
|
Description
:
|
Calcium concentrations measured by inductively coupled plasma optical emission spectroscopy (ICP-OES, Agilent 5100 VDV OES, Agilent, Waldbronn, Germany). |
|
Instrumentation:
|
Instrument:
Description:
|
Instrument: ICP-OES
|
Vendor: Agilent
|
|
|
|
Kw_pcp
--
Potassium measured in precipitation
|
Milligram per liter |
Potassium measured in precipitation time series |
|
Method
(Sampling/processing description of the values of
this attribute by one ore more steps.)
|
|
--- Step
1
---
|
|
Title
:
|
Measurement of potassium concentrations by ICP-OES |
|
Description
:
|
Potassium concentrations measured by inductively coupled plasma optical emission spectroscopy (ICP-OES, 5100 VDV OES, Agilent, Germany). |
|
Instrumentation:
|
Instrument:
Description:
|
Instrument: ICP-OES
|
Vendor: Agilent
|
|
|
|
Mgw_pcp
--
Magnesium measured in precipitation
|
Milligram per liter |
Magnesium measured in precipitation time series |
|
Method
(Sampling/processing description of the values of
this attribute by one ore more steps.)
|
|
--- Step
1
---
|
|
Title
:
|
Measurement of magnesium concentrations by ICP-OES |
|
Description
:
|
Magnesium concentrations measured by inductively coupled plasma optical emission spectroscopy (ICP-OES, 5100 VDV OES, Agilent, Germany). |
|
|
Naw_pcp
--
Sodium measured in precipitation
|
Milligram per liter |
Sodium measured in precipitation time series |
|
Method
(Sampling/processing description of the values of
this attribute by one ore more steps.)
|
|
--- Step
1
---
|
|
Title
:
|
Measurement of sodium concentrations by ICP-OES |
|
Description
:
|
Sodium concentrations measured by inductively coupled plasma optical emission spectroscopy (ICP-OES, 5100 VDV OES, Agilent, Germany). |
|
Instrumentation:
|
Instrument:
Description:
|
Instrument: ICP-OES
|
Vendor: Agilent
|
|
|
|
NH4w_pcp
--
Ammonium measured in precipitation
|
Milligram of nitrogen per liter |
Ammonium measured in precipitation time series |
|
Method
(Sampling/processing description of the values of
this attribute by one ore more steps.)
|
|
--- Step
1
---
|
|
Title
:
|
Measurement of ammonia concentrations |
|
Description
:
|
Concentrations of ammonium-N (NH4-N) measured by continuous flow analysis (CFA) using high resolution colorimetry and photometric detection. During the CFA measurements, samples were dialyzed on-line and NH4-N was determined by the Berthelot reaction. Ammonia is buffered and chlorinated to monochloramine which reacts with salicylate to 5-aminosalicylate. After oxidation and oxidative coupling a green coloured complex is formed. The absorption of the formed complex is measured at 660 nm. |
|
Instrumentation:
|
Instrument:
Description:
|
Instrument: Continuous Flow Analyzer
|
Vendor: Seal, Norderstedt and Skalar, Breda
|
|
|
|
NO3w_pcp
--
Nitrate measured in precipitation
|
Milligram of nitrogen per liter |
Nitrate measured in precipitation time series |
|
Method
(Sampling/processing description of the values of
this attribute by one ore more steps.)
|
|
--- Step
1
---
|
|
Title
:
|
Measurement of nitrate concentrations |
|
Description
:
|
Nitrate-N (NO3-N) measured by continuous flow analysis (CFA) using high resolution colorimetry and photometric detection. After on-line dialysis, the sample is buffered at pH 8.2 and is passed through a column containing granulated copper-cadmium to reduce the nitrate to nitrite, which is determined by diazotizing with sulfanilamide and coupling with N-(1-naphthyl)ethylenediamine dihydrochloride to form a highly coloured azo dye which is measured at 540 nm. The determination of NO3-N concentrations by cadmium reduction usually includes a small amount of originally present nitrite-N (NO2-N), which was below the detection limits and hence considered negligible. |
|
Instrumentation:
|
Instrument:
Description:
|
Instrument: Continuous Flow Analyzer
|
Vendor: Seal, Norderstedt and Skalar, Breda
|
|
|
|
Ntotw_pcp
--
Total nitrogen measured in precipitation
|
Milligram of nitrogen per liter |
Total nitrogen measured in precipitation time series |
|
Method
(Sampling/processing description of the values of
this attribute by one ore more steps.)
|
|
--- Step
1
---
|
|
Title
:
|
Measurement of total nitrogen concentrations |
|
Description
:
|
Concentrations of total dissolved nitrogen (TN) measured by continuous flow analysis (CFA) using high resolution colorimetry and photometric detection. During the CFA measurements TN was oxidized to nitrate by UV digestion with potassium peroxydisulfate and sodium hydroxide in presence of a boric acid buffer. After dialysis the nitrate is reduced to nitrite by a cadmium copper reductor. The nitrite is determined by the Griess reaction, the colour is measured at 540 nm. |
|
Instrumentation:
|
Instrument:
Description:
|
Instrument: Continuous Flow Analyzer
|
Vendor: Seal, Norderstedt and Skalar, Breda
|
|
|
|
Stotw_pcp
--
Total sulphur measured in precipitation
|
Milligram per liter |
Total sulphur measured in precipitation time series |
|
Method
(Sampling/processing description of the values of
this attribute by one ore more steps.)
|
|
--- Step
1
---
|
|
Title
:
|
Measurement of sulphur concentrations |
|
Description
:
|
Sulphur concentrations measured by ICP-OES |
|
Instrumentation:
|
Instrument:
Description:
|
Instrument: ICP-OES
|
Vendor: Agilent
|
|
|
|
Clw_pcp
--
Chloride measured in precipitation
|
Milligram per liter |
Chloride measured in precipitation time series |
|
Method
(Sampling/processing description of the values of
this attribute by one ore more steps.)
|
|
--- Step
1
---
|
|
Title
:
|
Measurement of chloride concentrations |
|
Description
:
|
Chloride measured in acqueous samples by continuous flow analysis (CFA) and ion-selective electrode (ISE). |
|
Instrumentation:
|
Instrument:
Description: Measurement of Cl concentration by continuous flow analysis (CFA) and ion selective electrode (ISE) in presence of an ionic strength adjustment buffer (NaNO3)
|
Instrument: Continuous Flow Analyzer / Ion selective electrode
|
Vendor: Seal, Norderstedt and Skalar, Breda / ThermoFisher, Beverly
|
|
|
|
DOCw_pcp
--
Dissolved organic carbon measured in precipitation
|
Milligram per liter |
Dissolved organic carbon measured in precipitation time series |
|
Method
(Sampling/processing description of the values of
this attribute by one ore more steps.)
|
|
--- Step
1
---
|
|
Title
:
|
Measurement of total organic carbon concentrations |
|
Description
:
|
Total organic carbon (TOC) measured as non-purgeable organic carbon (NPOC) by elemental analysis through high temperature combustion and infrared (IR) detection (varioTOC cube, elementar Analysensysteme GmbH, Hanau, Germany), after acidifying 10 mL of the sample with 50 µL of a 10% HCl solution to remove inorganic C. |
|
Instrumentation:
|
Instrument:
Description:
|
Instrument: Elemental Analyzer (liquid mode)
|
Vendor: Elementar Analysensysteme, Hanau
|
|
|
|
PO4w_pcp
--
Ortho-phosphate (reactive phosphorus) measured in precipitation
|
Milligram of phosphorus per liter |
Ortho-phosphate (reactive phosphorus) measured in precipitation time series |
|
Method
(Sampling/processing description of the values of
this attribute by one ore more steps.)
|
|
--- Step
1
---
|
|
Title
:
|
Measurement of phosphate concentrations |
|
Description
:
|
Concentrations of orthophosphate (oPO4-P) measured by continuous flow analysis (CFA) using high resolution colorimetry and photometric detection. Ammonium heptamolybdate and potassium antimony(III) oxide tartrate react in an acidic medium with dialysed and diluted solutions of phosphate to form an antimony-phospho-molybdate complex. This complex is reduced to an intensely blue-coloured complex by L(+)ascorbic acid. The complex is measured at 880 nm. |
|
Instrumentation:
|
Instrument:
Description:
|
Instrument: Continuous Flow Analyzer
|
Vendor: Seal, Norderstedt and Skalar, Breda
|
|
|
|
Ptotw_pcp
--
Total phosphorus measured in precipitation
|
Milligram of phosphorus per liter |
Total phosphorus measured in precipitation time series |
|
Method
(Sampling/processing description of the values of
this attribute by one ore more steps.)
|
|
--- Step
1
---
|
|
Title
:
|
Measurement of total phosphorus concentrations |
|
Description
:
|
Concentrations of total dissolved phosphorus (TP), measured by continuous flow analysis (CFA) using high resolution colorimetry and photometric detection. The sample is mixed with a potassium peroxodisulfate and organic phosphates are destructed by means of UV digestion. Sulfuric acid is added to the sample stream and the solution and complex inorganic phosphates are digested at 110 °C to ortho-phosphate. Sodium hydroxide is added to neutralise the solution which is dialysed against distilled water. Ammonium heptamolybdate catalysed by potassium antimony(III) oxide tartrate reacts in an acidic medium with diluted solutions of phosphate to form a phospho-molybdic acid complex. This complex is reduced in an intensely blue colored complex by L(+)ascorbic acid. This complex is measured at 880 nm. |
|
Instrumentation:
|
Instrument:
Description:
|
Instrument: Continuous Flow Analyzer
|
Vendor: Seal, Norderstedt and Skalar, Breda
|
|
|
|
